電解池作(zuo)過一至二百(bai)個樣(yang)品后，應(ying)重新處理，否則將直接影響氫值的分析結果，使氫值偏低(di)，處理方法如下：

  (1) 卸(xie)下電解池；

  (2) 清洗(xi)(xi)(xi)電(dian)解池：首先用(yong)(yong)(yong)自來水(shui)將其(qi)沖(chong)(chong)洗(xi)(xi)(xi)，然后用(yong)(yong)(yong)小軟毛刷(shua)沾上洗(xi)(xi)(xi)衣粉，慢(man)慢(man)向左向里旋(xuan)動毛刷(shua)，注意旋(xuan)動到引(yin)線即可，再(zai)(zai)慢(man)慢(man)地向右向外旋(xuan)動毛刷(shua)退出，用(yong)(yong)(yong)水(shui)沖(chong)(chong)洗(xi)(xi)(xi)，看鉑絲是否洗(xi)(xi)(xi)亮，如發現有(you)黑(hei)處，可重新(xin)用(yong)(yong)(yong)毛刷(shua)刷(shua)洗(xi)(xi)(xi)直到洗(xi)(xi)(xi)凈，最(zui)后用(yong)(yong)(yong)蒸餾(liu)水(shui)沖(chong)(chong)洗(xi)(xi)(xi)干(gan)凈，再(zai)(zai)用(yong)(yong)(yong)丙銅沖(chong)(chong)洗(xi)(xi)(xi)一下，完(wan)畢后，用(yong)(yong)(yong)電(dian)吹風(熱風檔) 吹干(gan)，接著用(yong)(yong)(yong)萬用(yong)(yong)(yong)表電(dian)阻擋(2K) 量(liang)電(dian)解池兩極，內阻應(ying)量(liang)無窮大，表明清洗(xi)(xi)(xi)完(wan)好，否則重新(xin)清洗(xi)(xi)(xi)。

  (3) 配電解液：取10ml或15ml的小量(liang)筒，按(an)體積比先盛(sheng)(sheng)入3份(fen)磷酸(優級純)，再盛(sheng)(sheng)入7份(fen)丙(bing)銅，輕搖量(liang)筒，筒底(di)應(ying)有(you)熱量(liang)散發。 

  (4) 涂(tu)    膜：將洗清好(hao)的電(dian)解(jie)(jie)池粗端傾斜向(xiang)上(shang)，把配好(hao)的電(dian)解(jie)(jie)液(ye)(ye)向(xiang)電(dian)解(jie)(jie)池內倒，第(di)一(yi)次到(dao)至(zhi)電(dian)解(jie)(jie)池長(chang)度的1/2 (若電(dian)解(jie)(jie)液(ye)(ye)還向(xiang)下流，應將其(qi)放平，用濾紙(zhi)擦(ca)凈流過(guo)來的電(dian)解(jie)(jie)液(ye)(ye)),然(ran)后用冷風吹(chui)干(gan)，第(di)二次倒至(zhi)電(dian)解(jie)(jie)池全部 (注意不要(yao)流過(guo)兩極) ，再(zai)用冷風吹(chui)干(gan)，第(di)三次倒入(ru)一(yi)半，用冷風吹(chui)干(gan)，然(ran)后用萬用表(1Ω擋)量兩極，如有(you)一(yi)定的阻值(幾歐或幾十歐)，則涂(tu)膜正常，否則重涂(tu)。

  (5) 裝(zhuang)上涂(tu)膜好(hao)的電(dian)解(jie)池(chi)，并將冷卻套裝(zhuang)上，使(shi)電(dian)解(jie)池(chi)細端略微(wei)向上傾斜。

  (6) 電(dian)(dian)(dian)(dian)解：打開氣路(lu)，流量計顯(xian)示80mL／min，開啟電(dian)(dian)(dian)(dian)源，按下涂膜鍵，60分鐘后電(dian)(dian)(dian)(dian)解至(zhi)終(zhong)點(dian)，可再(zai)按涂膜鍵，繼續涂膜，直到終(zhong)點(dian)(電(dian)(dian)(dian)(dian)解流≤70mA)，到達(da)終(zhong)點(dian)后，可按“月、日”鍵，分別(bie)按入單數(shu)和雙(shuang)數(shu)，再(zai)按返回鍵使電(dian)(dian)(dian)(dian)解電(dian)(dian)(dian)(dian)流能(neng)快速降至(zhi)終(zhong)點(dian)，如此反復多(duo)次，即可使用。至(zhi)此電(dian)(dian)(dian)(dian)解池(chi)處理完畢，做正式(shi)樣(yang)前先(xian)分析兩個廢樣(yang)以(yi)平(ping)衡系統(tong)。