煤質工業分析儀的實驗過程
2024-08-16 來(lai)自(zi): 鶴壁市科達儀(yi)器儀(yi)表有限公(gong)司(si) 瀏覽(lan)次(ci)數:484
全自動工業分析儀是一(yi)種(zhong)工業用儀器(qi)。用來測(ce)試水分、灰分、揮發分三種(zhong)指標。
由分析儀、計算機系統、打印機三部分組成。其將遠紅外加熱設備與電子天平結合(he)在(zai)一(yi)起,在(zai)特定的(de)氣氛條件、規定的(de)時間內對受熱過(guo)程中的(de)試樣予以稱(cheng)重,以此(ci)計(ji)算(suan)出試樣的(de)水分(fen)、灰(hui)分(fen)及揮發分(fen)等工業分(fen)析指(zhi)標。實現水分(fen)、灰(hui)分(fen)、揮發分(fen)三項指(zhi)標間任意組合(he)測(ce)定或單獨測(ce)定,在(zai)150分(fen)鐘(zhong)內可以測(ce)試19個樣品的(de)水分(fen)、灰(hui)分(fen)、揮發分(fen)三項指(zhi)標。
煤炭工業分析儀的(de)實驗流(liu)程,進入(ru)工作測(ce)試(shi)菜單,輸入(ru)相(xiang)關的(de)試(shi)樣信息后儀(yi)器(qi)自動(dong)稱(cheng)量空坩(gan)(gan)堝(guo)(guo)(guo),空坩(gan)(gan)堝(guo)(guo)(guo)稱(cheng)量完(wan)畢,系(xi)統(tong)(tong)自動(dong)打(da)開(kai)上蓋,提示放入(ru)試(shi)樣,然后系(xi)統(tong)(tong)稱(cheng)量試(shi)樣質(zhi)(zhi)量并(bing)開(kai)始加(jia)熱。升(sheng)(sheng)溫(wen)(wen)到145℃左右(you)恒溫(wen)(wen)30分(fen)鐘(zhong)(指按國標(biao)方(fang)法,溫(wen)(wen)度(du)與恒溫(wen)(wen)時(shi)(shi)間可自定(ding)(ding)義設置)后開(kai)始稱(cheng)量坩(gan)(gan)堝(guo)(guo)(guo),當(dang)坩(gan)(gan)堝(guo)(guo)(guo)質(zhi)(zhi)量變化(hua)不超過(guo)系(xi)統(tong)(tong)設定(ding)(ding)值(默認0.0006克)時(shi)(shi)水分(fen)分(fen)析(xi)結(jie)束,系(xi)統(tong)(tong)報(bao)出水分(fen)測(ce)定(ding)(ding)結(jie)果(guo)(guo),此(ci)時(shi)(shi)系(xi)統(tong)(tong)會(hui)(hui)自動(dong)打(da)開(kai)上蓋,提示加(jia)坩(gan)(gan)堝(guo)(guo)(guo)蓋,儀(yi)器(qi)自動(dong)稱(cheng)量加(jia)坩(gan)(gan)堝(guo)(guo)(guo)蓋質(zhi)(zhi)量,然后系(xi)統(tong)(tong)控(kong)(kong)制高(gao)溫(wen)(wen)爐繼續(xu)升(sheng)(sheng)溫(wen)(wen),目標(biao)溫(wen)(wen)度(du)900℃(系(xi)統(tong)(tong)自動(dong)打(da)開(kai)氮氣(qi)閥(fa),向高(gao)溫(wen)(wen)爐內通氮氣(qi),氣(qi)體流(liu)量控(kong)(kong)制在(zai)4-5L/min),高(gao)溫(wen)(wen)爐溫(wen)(wen)度(du)升(sheng)(sheng)到900℃,恒溫(wen)(wen)規定(ding)(ding)的(de)時(shi)(shi)間后,系(xi)統(tong)(tong)會(hui)(hui)自動(dong)打(da)開(kai)上蓋開(kai)始降溫(wen)(wen),當(dang)高(gao)溫(wen)(wen)爐溫(wen)(wen)度(du)降到設定(ding)(ding)值時(shi)(shi),儀(yi)器(qi)自動(dong)稱(cheng)量各坩(gan)(gan)堝(guo)(guo)(guo)質(zhi)(zhi)量,系(xi)統(tong)(tong)報(bao)出揮發分(fen)測(ce)定(ding)(ding)結(jie)果(guo)(guo)。此(ci)時(shi)(shi)系(xi)統(tong)(tong)再次升(sheng)(sheng)溫(wen)(wen)至845℃恒溫(wen)(wen)(系(xi)統(tong)(tong)會(hui)(hui)打(da)開(kai)氧氣(qi)閥(fa),向高(gao)溫(wen)(wen)爐內通氧氣(qi),氣(qi)體流(liu)量控(kong)(kong)制在(zai)4-5L/min),之后系(xi)統(tong)(tong)開(kai)始稱(cheng)量坩(gan)(gan)堝(guo)(guo)(guo),當(dang)坩(gan)(gan)堝(guo)(guo)(guo)質(zhi)(zhi)量變化(hua)不超過(guo)系(xi)統(tong)(tong)設定(ding)(ding)值(默認0.0006克)時(shi)(shi)灰分(fen)分(fen)析(xi)結(jie)束,系(xi)統(tong)(tong)報(bao)出灰分(fen)測(ce)定(ding)(ding)結(jie)果(guo)(guo),并(bing)打(da)印(yin)結(jie)果(guo)(guo)或(huo)報(bao)表(如果(guo)(guo)在(zai)系(xi)統(tong)(tong)設置中設置了打(da)印(yin))。